Acta naturalia Islandica - 01.07.1964, Page 12

Acta naturalia Islandica - 01.07.1964, Page 12
10 SIGURDUR STEINTHÓRSSON A four-axes Universal stage was employed to determine the angle 2H of olivines, pyroxenes and few plagioclase crystals. The maximum extinction angle of pyroxene, and the parallel (max.) extinction angles of plagioclase were also determined by this means. It was attempted to use the methods of Köhler and Reinhard to determine the An-content of the plagioclase, but too' much zoning rendered the methods impracticable. The cores of the phenocrysts, how- ever, could be determined in this way giving (a) the composition, (b) the nature (high temperature) and (c) the twin law. For the groundmass plagio- clase the zone method of Rittmann was employed in conjunction with refractive index. The rock was ground down, the feldspars separated in heavy liquid (bromoform) and maximum and minimum R.I. found in sodium light by the immersion method and a Leitz-Jelley refractometer. The accuracy is estimated as ± 0.003, but might be less in certain cases because of the possiblity that the actual maximum or minimum values were not obtained from the randomly orientated grains. By comparing the R.I. values with the ones obtained fram the extinction angles the groundmass crystals were found to be high tempera- ture plagioclase as well. Direct measurements of 2V of olivines and pyroxenes were made when- ever possible. They were corrected for difference in R.I. between hemispheres and the mineral according to the formula p sinV = n sinH. The measurements were orthoscopic. The R.I. of the hemispheres used was n = 1.557 in all cases. The R.I. of the central plate is n= 1.560. The majority of the measurements was made With U.M. 2 objective and fully open diaphragm (Munro 1963). The maximum possible error in actual reading of 2H is estimated ± 1° (0.5° on each side), but the accuracy may be as small 'as ±3° in the case of olivine corresponding to 6% Fa. The pyroxene measurements are more accurate due their smaller optic axial angles, or ± 1.5°. Measurements of R.I. of olivine and pyroxene were made on orientated sections giving np. The accuracy in estimated ± 0.003. The values thus obtained correspond reasonably well with those obtained from the 2Vs. The carbonate present in the rock was determined by X-ray powder method as aragonite. One olivine crystal was determined in this way as well, and was found to be Fo 83%, Fa 17%. (Yoder 1957). Modal analysis was made of representative sections. About 1000 points were counted in each section. A fine interval eounter was used in most cases (10 points per mm), but a coarser one (3 points per mm) was used to count some of the coarser grained sections. The modes were determined for (a) com- position of the groundmass, (b) phenocrysts, and (c) overall composition. The density of numerous specimens wias measured by means of a Walker’s

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Acta naturalia Islandica

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